Studies on natural p-terphenyls: total syntheses of vialinin A and terrestrin B.

نویسندگان

  • Yue Qi Ye
  • Hiroyuki Koshino
  • Jun-ichi Onose
  • Kunie Yoshikawa
  • Naoki Abe
  • Shunya Takahashi
چکیده

A powerful inhibitor of TNF-alpha production, vialinin A, was synthesized from sesamol through a series of reactions involving double Suzuki-Miyaura coupling, 2,3-dichloro-5,6-dicyano-1,4-benzoquino (DDQ) mediated de-methoxymethylation and oxidative removal of methylene acetal by lead tetraacetate. The synthetic method also made it possible to prepare a related compound, terrestrin B.

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عنوان ژورنال:
  • Bioscience, biotechnology, and biochemistry

دوره 74 1  شماره 

صفحات  -

تاریخ انتشار 2010